M. D'ERCOLE Stefano

PhD Student Team FunSurf- Supervised by David Munoz-Rojas
LMGP Grenoble-INP, Minatec 3, parvis Louis Néel CS 50257 38016 Grenoble Cedex 1 France
1-20
0456529346
Contact e-mail

Deposition of thin-films of semiconductor oxides (ex., Ag2O, NiO,...) via Spatial Atomic Layer Deposition (SALD) for opto-electronic applications. 
Characterisation techniques:

  • X-Ray Diffraction (XRD): crystal structure, phase identification
  • X-ray Photoelectron Spectroscopy (XPS): surface chemistry, oxidation state.
  • Fourier Transfrom Infra-Red (FTIR) and Raman spectroscopies: identification of molecules and detection of residual ligands/precursor molecules.
  • Ultra Violet-Visible spectroscopy (UV/Vis): analysis of sample's transmittance and derivation of its bandgap.
  • Scanning Electron Microscope (SEM): surface morphology of the samples.
  • Energy Dispersive X-ray diffraction (EDX): Identification of chemical species present in the sample.
Other instruments used:
  • 3D printing/CAD: Fusion 360 to design components which are then 3D printed (mainly Stereolitography).
  • Thermogravimetric Analysis (TGA): to analyse the thermal stability of the precursors and to analyse precursor's evaporation over time at constant temperature (Iso-TGA) .